1. Use the CCD camera (
NMR-MX5; see
section (INSERT LINK TO
ON LINE CAMERA MANUAL HERE)) to obtain an image of
the back side of the ladder at the sample position (be sure
that the program is receiving the signal from the polarimeter
camera). The torus of LCD lights surrounding the camera will
probably need to be illuminated to provide sufficient
background light for an image. Or, the cover plates at
the end of this section of the beam line may be removed to
introduce ambient light. Using the photometry tool (View >
Photometry)
determine the (x,y) co-ordinate that corresponds to the center of
newly loaded sample.
2. Open (File
Load) the most recent stored image of the
polarimeter beam-spot taken with sapphire in the sample
position (see below). Using the photometry tool determine
the (x,y) co-ordinate that corresponds to the center of
the beam spot. Elements of the beam line may be 'tweaked'
during the course of experiments, so be sure to use the most
recent image. The co-ordinates of the center should also be
recorded in the bNQR logbook.
[If you are unsure of the exact co-ordinates, you may want to
place the sapphire in the sample position (part A above),
have the beamstop removed, and image the beam-spot with the
camera (no additional light required).]
3. Compare the co-ordinates for the center of the present
sample with those of the beam-spot image. Determine if the
sample should be raised or lowered (or neitrher) relative
to the beam-spot. Using the remote control for the motor,
drive the entire cryostat 'UP" or 'DOWN' as desired. Small,
incremental changes are recommended. (Be careful, depending
on the orientation of the CCD camera, UP and DOWN may be reversed!).
4. Re-image the sample after cryostat adjustment and continue
to adjust as needed.
Next:Getting out a sample Up:Changing and aligning samples Previous:Lateral AlignmentContents
BNMR Web Site
2006-06-29