(b) Allen wrench
adjusting the top-right screw of the cryostat alignment
(c)
CCD camera
(d)
Halogen lamp used in lightning the Cryostat with its DC power supply
(a) Bad
(b) good alignment of the cryostat
4.1We have noticed that the cryostat dis-aligns each time
after mounting a sample. So, it is very practical to take a
flash-light picture after each mounting to make sure that the cryostat
did not move. To do that place the flash-light in-lieu of cover of the
hole close to the telescope. Connect the camera to the computer with
appropriate wire (labeled BNMR).
Take a picture of the cryostat with the flash-light on (don't forget to
turn it off after you are done with it)
using a time exposure of
0.1 sec, and see if the
sample holder is in the middle
of the bright flash-light circle
(black circle as in Fig. 4.1-a). If it is
shifted from the center,
then adjusting the cryostat is mandatory. Loosing or tightening the
screws of the cryostat is the way to get it centered (see Fig. 4.1).
The screws to adjust are shown in Fig. 4.1, and rotating the top
or bottom ones (two sizes small and bigger,
each with two in front and two in the
bottom with a square drive)
in 45
using an Allen wrench
is enough to make the cryostat move up or
down (3-4mm). There are 4 locking screws (big one in picture)
that must first first loosened with an 5/32 Allan wrench.
The small screws ( where Allan wrench, size 3/32,
in figure is pointed) can move
the cryostat by
2mm for half turn. Adjusting these screws must
be experienced by small turns and taking pictures with CCD camera.
After adjustment you should be able to center the
cryostat and get a picture similar to Fig.4.1-b.
A more robust and time
consuming way would be using the telescope, which is explained next.
Next:With the telescope Up:Alignment of the cryostat Previous:Alignment of the cryostatContents
BNMR Web Site
2006-06-29